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Low Energy Ball Milling

Simple and efficient solid-state synthetic methods, aging and ball milling (liquid-assisted grinding, LAG), have been employed to achieve reactions of triphenylphosphine (tpp) and 1,1′-bis(diphenylphosphino)ferrocene (dppf) with dicyclopalladated azobenzenes (DMF)PdCl(μ-R1C6H3N═NC6H3R2)PdCl(DMF), R1 = H, OCH3, N(CH3)2 and R2 = H, NO2. For the first time the …

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